Download Lipid analysis and lipidomics : new techniques and by Magdi M Mossoba PDF

By Magdi M Mossoba

Content material: strategy and purposes in lipid research / NIls Hinrichsen and Hans Steinhart -- an outline of contemporary mass spectrometry equipment within the toolbox of lipid chemists and biochemists / R. Moreau -- worldwide mobile lipidome analyses via shotgun lipidomics utilizing multidimensional mass spectrometry / X. Han and R.W. Gross -- LC/MS and chiral separation / A. Kuksis and Y. Itabashi -- LC/MS and lipid oxidation / A. Kuksis and O. Sjovall -- Structural research of unsaturated fatty acid methyl ester isomers with acetonitrile covalent adduct chemical ionization (CACI) / J.T. Brenna -- contemporary advances in silver-ion HPLC using acetonitrile in hexane as solvent: temperature results on lipid elution orders/resolution / R.O. Adlof -- research of trans-18:1 fatty acids by means of silver ion HPLC / P. Delmonte, J.K.G. Kramer, and M.P. Yurawecz -- High-performance size-exclusion chromatography for lipid research in natural media / G. Márquez-Ruiz and M.C. Dobarganes -- Lipid separations utilizing packed-column supercritical fluid chromatography / D.G. Hayes --TLC-FID with specified connection with marine lipids and different high-molecular-weight natural compounds / R.G. Ackman and A. Timmins -- speedy GC for mobile status research of micro organism / J.S. consumer. Use of mobile fatty acids to spot food-borne pathogens by way of infrared spectroscopy and capillary fuel chromatography / M.M. Mossoba and S.F. Al-Khaldi -- program of FT-NIR for quick selection of the trans fatty acid composition in fat and oils / H. Azizian and J.K.G. Kramer -- Infrared spectroscopy and partial least sq. calibration within the simultaneous quantification of remoted trans and conjugated linoleic acids / A.A. Christy -- research of protein-lipid interactions by way of vibrational spectroscopy / G. Meng, N.K. Howell, and E.C.Y. Li-Chan -- fats replacers: an summary / W.E. Artz, S.M. Mahungu, and S.L. Hansen -- Phospholipids: constructions and physicochemical actions / M.C. Erickson -- Waxes and sterols: constructions and chemistry / E.J. Parish and A.D. Bell

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Html (accessed January 2005). 4. , Gas Chromatography—Mass Spectrometry Methods for Structural Analysis of Fatty Acids, Lipids 33:343–353 (1998). 5. , A. Nunez, and V. Singh, Diferuloylputrescine and p-Coumaroylferuloylputrescine, Abundant Polyamine Conjugates in Lipid Extracts of Maize Kernels, Lipids 36:839–844 (2001). 6. , Electron Impact Ionization Mass Spectrometry as a Tool for LC/MS Analysis of Lipids and Derivatives, INFORM 12:502–509 (2001). 7. T. A. F. R. D. Jones, Hopanoid Lipids Compose the Frankia Vesicle Envelope, Presumptive Barrier of Oxygen Diffusion to Nitrogenase, Proc.

Due to the recent develop51 Copyright (c) 2006 by AOCS Press Chapter03 2/25/06 12:49 PM 52 Page 52 X. W. Gross ment of various soft ionization techniques such as electrospray ionization (ESI), matrix-assisted laser desorption/ionization (MALDI), and atmospheric pressure chemical ionization (APCI), MS has emerged as the preferred physical method for the profiling of the cellular lipidomes [see (1,3,5–11) for recent reviews]. Among these mass spectrometric techniques, ESI-MS is the most prominent and has enjoyed the most success.

11A). By scanning at a preselected radio frequency, one effectively scans a particular mass range. Quadrupoles are the least expensive and most popular mass analyzers for ESI, APCI, and APPI MS. Copyright (c) 2006 by AOCS Press Chapter02 2/25/06 12:44 PM Page 45 Modern Mass Spectrometry Methods 45 Fig. 11. Methods of mass analysis (ion separation). (A) Quadrupole; (B) ion trap; (C) time of flight; (D) tandem mass spectrometry (MS). Figure provided by A. Nuñez. A. Moreau Quadrupole ion trap mass analyzers “trap” ions in a radio frequency quadrupole field.

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