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By Anil K. Mukherji, R. Belcher and M. Frieser (Auth.)

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32, 687 (1955). 60. R A Y , A. K. , Sei. and Culture (India), 21, 437 (1956). 61. D H A R , S. K. and D A S GUPTA, A. , / . Sei. Ind. Research (India), 11B, 500 (1952). 62. , and MOLDOVEANU, J. Rev. Chim. Acad. Rep. Populaire 63. 64. 65. 66. 67. 68. 69. 70. 71. 72. Rumania, 7, 375 (1962). Chem. Abstracts, 59, 2164C (1963). SUBANNA, V. V. and BHATTACHARYA, A. , Anal. Chim. Acta, 23, 145 (1960). SRIVASTAVA, T. , Z . Anal. Chem. 169, 254 (1959). AGRAWAL, S. , Z . Anal. Chem. 171, 91 (1960). , Z . Anal.

25, 421 (1903). 29. , Z . Anal. Chem. 78, 133 (1929); 86, 13 (1931). 30. RAY, P. and CHATTOPADHYA, A. , Z . Anorg. Chem. 169, 199 (1926). 31. HOLNESS, H . and KEAR, R. , Analyst, 74, 597 (1949). 32. PURUSHOTTAM, A. and RAGHAVA R A O , B. S. , Analyst, 75, 555 (1950). 33. PURUSHOTTAM, A. and RAGHAVA RAO, B. S. , Rec. Trav. Chim. 70,555 (1951). 34. SCHOELLER, W. , Analyst, 58, 132 (1933); 61, 585 (1936). 35. SCHOELLER, W. R. and POWELL, A. , Analysis of Minerals and Ores of the Rarer Elements, 3rd edn, Hafner, New York, 1955.

Note. (1) Loss of volume in the depolymerization digestion is immaterial. Evaporation to fumes is equally effective. (2) 100 milliequivalents of sulfuric acid is a desirable maximum. Prior evaporation of an aliquot, if necessary, to establish around 5 N acidity is preferable to using any excess acid. (3) Titration with EDTA should be commenced at an acidity not less than 2 N for amounts of zirconium above 60 mg in order to avoid depolymerization. 2, yielding a sharp endpoint. 5 %. (5) Sinha and Das Gupta(44) and Pilkington and Wilson(35) do not agree on the depolymerization action of sulfuric acid.

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